By P. W. Selwood
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Additional resources for Chemisorption and Magnetization
Magnet assembly for measurement of M 8 at low temperatures. 36 III. M E A S U R E M E N T S AT HIGH M~MQ avoid damage to the sensing coils. A small sleeve furnace provides the proper reduction temperature. T h e gas handling system is also of conventional design as shown in Fig. 12. In brief, the sample is reduced b y flowing purified hydrogen for m a n y hours. For a typical nickel-silica sample the reduction temperature is 633 K . T h e sample is then evacuated for a minimum of 2 hours at 633 Κ to a -4 - 2 pressure of about Ι Ο Ν « m , and allowed to cool to the temperature of measurement.
Rauch, and V . Wilderspaner, J. Phys. Chem. Solids 31, 391 (1970) W . F . Brown, / . Appl. Phys. 30, 130S (1959). P. O . Voznyuk and V. N . Dubinin, Ukr. Fiz. Zh. 19, 160 (1974). J. L . Carter and J. H . Sinfelt, Catal. 10, 134 (1968). J. L . Carter, J. A . Cusumano, and J. H . Sinfelt, J. Phys. Chem. 70, 2257 (1966). III Magnetization Measurements at High M/Mo 1. The Experimental Problem Our chief purposes are to show h o w magnetic methods m a y b e used t o measure particle size and t o gain information concerning the binding of an adsorbate t o an adsorbent.
Carter, J. A . Cusumano, and J. H . Sinfelt, J. Phys. Chem. 70, 2257 (1966). III Magnetization Measurements at High M/Mo 1. The Experimental Problem Our chief purposes are to show h o w magnetic methods m a y b e used t o measure particle size and t o gain information concerning the binding of an adsorbate t o an adsorbent. One m e t h o d of achieving the latter goal is, in appropriate systems, t o measure the change in average magnetic m o m e n t of adsorbent atoms per molecule of vapor adsorbed.
Chemisorption and Magnetization by P. W. Selwood